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Methods by FLAA:
 
Flame AA Methods and Sample Types
NIOSH 7082 (Aug 1994), OSHA ID-121
Metal:  Pb
Matrix: Airborne Dust Samples
Filter: 0.8 mm cellulose ester membrane, 37-mm Cassettes
Flow rate: 1 to 4 L/min
Volume: 200-1500 L
Reporting units: mg/ m3
MDL: 10 mg/sample
Regulatory Limits:
OSHA (general industry): 50 mg/m3
OSHA (construction): 200 mg/m3
OSHA-action level (TWA): 30 mg/m3
NIOSH: < 100 mg/ m3
TWA upon request

NIOSH 7082M (Aug 1994)
Metal:  Pb
Matrix: Dust Wipe
Wipe: Rite-Aid Baby Wipe, Ghost Wipe
MDL: 10 mg/sample
Regulatory Limits:
HUD clearance level for floor: 200 mg/ft2
HUD clearance level for window sill: 500 mg/ft2
HUD clearance level for window well: 800 mg/ft2
Reporting units: mg/ sample, mg/ft2
mg/cm2 and mg/cm2 upon request

Paint Chips
Digestion Method: ASTM E 1645-01 or EPA 3050A
Analytical Method: EPA 7420, EPA 6010
Minimum material needed: 0.1 g
MDL: 0.01 percent weight, 50 mg/Kg (ppm)
Regulatory Limits:
HUD: 5000 ppm or 0.5 weight percent
OSHA: 600 ppm or 0.06 weight percent
Reporting units: mg/Kg, ppm or weight percent
mg/cm2 will be provided upon request.

Soil and Solid Waste
Analytical Method: EPA 7420 or EPA 6010
Minimum material needed: 5.0 g
MDL: 2.0 mg/Kg (ppm)
Regulatory Limits:
TTLC: 1000 mg/Kg (ppm)
STLC: 5.0 mg/L (ppm)
Reporting units: mg/Kg, ppm

Waste Water
Analytical Method: EPA 7420, SM 3111b or C, EPA 239.1
Minimum material needed: 250 mL
MDL: 0.1 mg/L (ppm)
Regulatory Limits:
TTLC: 1000 mg/Kg (ppm)
Reporting units: mg/L (ppm)

 
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